![]() The Journal of Physical Chemistry Letters 2023, 14 Spinel-Derived Formation and Amorphization of Bimetallic Oxyhydroxides for Efficient Electrocatalytic Biomass Oxidation. Fangyuan Wang, Yuming Gu, Bailin Tian, Yuxia Sun, Lifeng Zheng, Shengtang Liu, Yiqi Wang, Lingyu Tang, Xiao Han, Jing Ma, Mengning Ding.Oxygen Evolution/Reduction Reaction Catalysts: From In Situ Monitoring and Reaction Mechanisms to Rational Design. Yonggui Zhao, Devi Prasad Adiyeri Saseendran, Chong Huang, Carlos A.Alkylamine-Confined Thickness-Tunable Synthesis of Co(OH)2-CoO Nanosheets toward Oxygen Evolution Catalysis. Chuansheng He, Linlin Yang, Xiaohui Peng, Shangheng Liu, Jia Wang, Chengyuan Dong, Delin Du, Leigang Li, Lingzheng Bu, Xiaoqing Huang.Industrial & Engineering Chemistry Research 2023, 62 Cobalt-Based Hydrotalcite: A Potential Non-Noble Metal-Based Heterogeneous Catalyst for Selective Hydrogenation of Aromatic Aldehydes. Padinjare Purayil Neethu, Ganesh Venkatachalam, Naragalu Javaregowda Venkatesha, Daisy Joseph, Ayyamperumal Sakthivel.The Journal of Physical Chemistry Letters 2023, Article ASAP. Insights into Chemical Changes Causing Transient Potential Patterns during Cobalt Electrodeposition: An Operando SHINERS Investigation. This article is cited by 1143 publications. This research has developed methodology for the synthesis of cobalt oxide and cobalt oxyhydroxide nanodiscs at low temperatures. The thermal stability of the materials Co(OH) 2 and CoO(OH) was established. Raman spectroscopy of the as-prepared Co(OH) 2, CoO(OH), and Co 3O 4 nanomaterials characterized each material. ![]() Bonding of the divalent cobalt hydroxide from the oxyhydroxide and oxides by studying their high-resolution XPS spectra for Co 2p 3/2 and O 1s. Characterization of these cobalt-based nanomaterials was fully developed, including X-ray diffraction, transmission electron microscopy combined with selected area electron diffraction, scanning electron microscopy, X-ray photoelectron spectroscopy, Raman spectroscopy, and thermal gravimetric analysis. Cobalt oxyhydroxide and cobalt oxide nanomaterials were synthesized through oxidation and low-temperature calcination from the as-prepared cobalt hydroxide. This morphology and nanosize is retained through to cobalt oxide Co 3O 4 through a topotactical relationship. The cobalt hydroxide displays hexagonal morphology with clear edges 20 nm long. Cobalt hydroxide, cobalt oxyhydroxide, and cobalt oxide nanomaterials were synthesized through simple soft chemistry.
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